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GCMS analysis results for sample AE06424, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE06424 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048776–000048792

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\APR04 05\6424.D Vial: 10 Acq On 5 Apr 2002 8:53 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

if leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 12.242 779 784 801 rBV 929678 2400641 69.46% 15.774% 2 14.849 1063 1068 1073 rVB 32585 64695 1.87% 0.425% 3 15.877 1174 1180 1198 rBV 1406268 3069275 88.81% 20.167% 4 21.183 1752 1758 1778 rBV 1616112 3456027 100.00% 22.708% 5 25.627 2236 2242 2255 rBV2 1456509 3154114 91.26% 20.725% 6 30.703 2790 2795 2802 rBV 159772 310771 8.99% 2.042% 7 33.687 3114 3120 3133 rBV2 746098 1656391 47.93% 10.884% 8 33.907 3140 3144 3153 rVB 36420 80919 2.34% 0.532% 9 37.928 3575 3582 3604 rBV2 340219 1026353 29.70% 6.744%

Sum of corrected areas: 15219186 6424.D GCMS0408.M Wed Apr 10 12:23:24 2002

NYC-WTC_000048789

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NYC-WTC_000048789Source: NYC Law Department, mirrored locally

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