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GCMS analysis results for sample AE06427, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE06427 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048810–000048826

Folder label: “GCMS X 4/11/02 A 4/15/02

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Scanned page image, NYC-WTC_000048823
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C: \HPCHEM\ 1 \DATA\APR04 05\6427.D Vial: 13 Acq On 6 Apr 2002 1:49 am Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 12.241 779 784 808 rVB 1017474 2658919 68.83% 15.432% 2 14.848 1060 1068 1073 rBV 21760 43922 1.14% 0.255% 3 15.885 1175 1181 1198 rBV 1583815 3395371 87.89% 19.706% 4 21.192 1752 1759 1772 rBV 1855143 3863104 100.00% 22.420% 5 25.635 2236 2243 2253 rBV 1644707 3563209 92.24% 20.680% 6 30.702 2790 2795 2804 rVB 168611 317073 8.21% 1.840% 7 33.686 3113 3120 3139 rBV2 864687 1995163 51.65% 11.579% 8 33.906 3139 3144 3154 rVB 40277 92309 2.39% 0.536% 9 37.927 3575 3582 3601 rBV2 430734 1301227 33.68% 7.552%

Sum of corrected areas: 17230297 6427.D GCMS0408.M Wed Apr 10 12:23:53 2002

NYC-WTC_000048823

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NYC-WTC_000048823Source: NYC Law Department, mirrored locally

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