GCMS unknown compound analysis, sample AE05512, March 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031702\5512.D Vial: 13 Acq On : 17 Mar 2002 6:35 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method j508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 I Min Area: 1 % of largest Peak Start Thrs: 0.2 I Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC peak R.T. first max last PK peakj corr. corr. % of # min scan scan scan TY ’ height area % max. total

1 5.570 272 275 295 rBV 150466 540347 5.17% 0.944% 2 9.543 708 713 732 rBV 2520455 6913673 66.19% 12.073% 3 12.046 985 989 1000 rVB 295588 555460 5.32% 0.970% 4 13.026 1091 1097 1111 rBV 4668287 9513174 91.08% 16.612% 5 18.132 1654 1660 1676 rBV 4986909 10333994 98.93% 18.045%

6 22.495 2134 2141 2154 rBV2 4757290 10445328 100.00% 18.240% 7 24.645 2374 2378 2388 rBV 75302 177481 1.70% 0.310% 8 27.429 2680 2685 2693 rBV 969786 1862005 17.83% 3.251% 9 30.305 2995 3002 3020 rBV 4083670 10269733 98.32% 17.933% 10 34.178 3423 3429 3449 rBV2 2559257 6656085 63.72% 11.623% 1 I Sum of corrected areas: 57267280

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:512.D 5080302.M Mon Mar 25 06:53:16 2002 Page 1 I

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