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GCMS unknown compound analysis, sample AE05697, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.

NYC-WTC_000059267–000059276

Folder label: “GCMS X 3/11/02 A 4/1/02

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Scanned page image, NYC-WTC_000059274
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO1O2\5697.D Vial: 12 Acq On 1 Apr 2002 11:09 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table , Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstCohc Area Relative to ISTD R.T.

8.13 3.00 ug/1 452184 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylfotmamide 73 C3H7NO 000627-45-2 9 2 Silane, ttfetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Diox<j61ane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Butane, -methoxy-2-methyl- , 102 C6H14O 000994-05-8 9 Abundance ......... I.................. ’ Scan'336 (8J 30 mln): 56977d (-) m/ z 73.00 100.00% 7b

5000 43

..................................37, L I 55. 67, I 87 103 7.80 8.00 8.20 8.40 m/ z 43.05 29.15%

L nite-> 10 20 30 40 50 60 70 80 90 100 110 -120 Abundance #292; N-Ethylformamide 3i0 73

5000 58 ■ 7.80 8.00 8.20 8.40 44 m/z 41.0,0 10.21%

m/z-> 10 1,5 20 4 4....... 'lil ' I '-'-'-I I " " I ' 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetraniefhyl- 73

7.80 8.00 8.20 8.40 5000 m/ z 9.59%

I 45 5 15 ;..... 66 , , , , ......... ' I ' ' ' Q”’ ’ ' ' I • ^/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423:1.3-Dioxolane, 2-{3-bromo-5,5.5-trichloro-2,2-dimet 7|3 7.80 8.00 8.20 8.40 m/z 71.0,0 6.16% SEH 45 3,6. Ill 55 67 I................................... ■ 'I' 10 20 30 40 50 60 70 80 90 100' 110 120 7 RO fl nn ft >n a in

5697.D GCMS0463.M Thu Apr 04 13:57:58 2002 Page 1

‘NYC-WTC_OOOO59274

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NYC-WTC_000059274Source: NYC Law Department, mirrored locally

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