GCMS analysis results, sample AE05237, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\5237.D Vial: 48 Acq On : 31 Mar 2002 3:35 pm Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area . Relative to ISTD R.T.

8.14 0.53 ug/1 62056 1,4-Dichlorobenzene-d4 12.25.

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pent^ol, 3-methyl- 102 C6H14O 000077-74-7 33 2 N-EthyJ^ormamide 73 C3H7NO 000627-45-2 9 3 Butane^ 2-methoxy-2-methyl- 102 C6H14O 000994-05-8 9 4 2-Me yl-1,5-pentanediamine 116 C6H16N2 _______ 015520-10-2 9 ■Abundance Scan337 (8.140 min): 5237.D (-) m/z 73.00 100.00% i 7|3

5000 43

, I, J 49 .,57 87 103 _J^:8g_J,00_jB;20_J,40L_^^ m/z 29.77% 'm/z-> 10 20 30___ 40_____ ^50___ 60_____ 70____ 80 90 100 110 'Abundance #63573: 3-Pentanol, 3-methyl- i 70 I

5000 .. .. ' I 7.80 8.00 8.20 !8.40 55 m/z 44.95 10.67% 27 45 87 39,I • < I’ ”t < ' I .1 m/2-> 10 20 30 40 50 60 70 80 90 100 110 Abundance

5000 30 #202. N-Ettiyiforrnsrnide

73 7.80 Js 8.00 41.05 8.20 8.40 8.88% 44 58

'm/z-> 10 20 30 40 50 60 70 80 90 100 110 ,, y IA4 A, I Abundance #1761: Butane. 2-methoxy-2-methyl- I 7|3 7.80 8.00 8.20 8.40 m/z 71.00 7.42% 5000 )i ft 55 87 i j ____ 27 33 ? I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' I \\ h 'm/z~> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5237.D GCMS0308.M Wed Apr 03 14:03:24 2002 Page 1

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