GCMS analysis results, sample AE05234, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5234.D Vial: 45 Acq On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator). Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Heptane, 4-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.40 0.76 ug/1 93602 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane,■4/methy1- 114 C8H18 000589-53-7 59 2 1-Butanol,/3-methyl - , acetate 130 C7H14O2 000123-92-2 42 3 Pentane, i-ethyl- 100 C7H16 000617-78-7 38 4 Pentane, l3 - ethyl - 2 -methyl - 114 C8H18 000609-26-7 38 Abundance 4)3 ' Scan 583 (10.401 nriin): 5234.b’G m/z. 4376p. ioo7ob%

5000 70

55 99 10.00 10.20 10.40 10.60 10.80 83 112 127 I .................'|l| ' I ' '''-I I ' m/z 20 30 40 50 60 70 80 90 100 110 120 130 iAbundance #3096: Heptane, 4-mefhyi- 43

71 5000 i 10.00 10.20 10,40 10.60 10.80 27 12.82% 1I 55 i I 40^ li II 65 114 20 30 50 60 70 80 90 100 110 120 130 Abundance #65212:1-Butanol, S-metlivi-. acetate 1 43

10.00 10.20 10.40 10.60 10.80 5000 70 m/z 41.05 12.17% 55

27 J”' 87 I 130 'n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 ■Abundance #1595; Pentane, 3-ethyl- T 10.00 10.20 10.40 10.60 10.80 m/z 42.00 11.84% 5000 70 29 55

rh/z--> ,-|-rn-,U|... I| 20 30 40 ,, J.. L... 50 60 70 80 90 100 100 iio 120 130 AA aA I 10.00 10.20 10.40 10 60 in fin

5234.D GCMS0308.M Wed Apr 03 13:59:20 2002 Page 3

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