Calibration data for pesticide analysis using method 508, showing compound response factors.
NYC-WTC_000057180–000057186Folder label: “508 X 11/15/01 A 12/12 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Signal 1 : C:\MSDCHEM\1\DATA\5O8\O11212B\PESTC2.D\ECD1A.CH Vial: 15 Signal 2 : C:\MSDCHEM\l\DATA\508\011212B\PESTC2.D\ECD2B.CH Acq On : 13 Dec 2001 8:44 am Operator: Nefliu Sample : pest ic2 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 26 14:12:16 2001 Quant Results File: 011212P.RES
Quant Method : C:\MSDCHEM\1\METHODS\011212P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 14:11:58 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M Volume Inj. Signal 1 Phase Signal #2 Phase: Signal 1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/1
System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.34 14.97 728.9E6 538.4E6 0.202m 0.200 Spiked Amount 0.200 Recovery = 101.00% 100.00% Target Compounds 1) Propachlor 9.05 8.49 94391858 68582999 0.191 0.191 2) g-BHC 9.82 10.18 2231.8E6 1683.2E6 0.283 0.293 3) Heptachlor 10.99 11.23 723.6E6 426.7E6 0.098 0.098 4) Aldrin 11.70 11.98 991.9E6 756.6E6 0.123 0.124 5) Heptachlor Epoxi 13.13 13.33 1699.OE6 1297.1E6 0.242 0.245 6) 4,4-DDE 13.96 14.54 2713.7E6 2127.9E6 0.404 0.410 7) Dieldrin 14.55 14.81 603.9E6 446.5E6 0.084 0.084 8) Endrin 15.05 15.46 1064.3E6 794.1E6 0.202 0.202 9) Methoxychlor 16.99 18.01 976.8E6 517.6E6 0.410 0.397
(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTC2.D 011212P.M Wed Dec 26 14:12:36 2001 Page 1
NYC-WTC_000057181
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NYC-WTC_000056440
Technical document displaying compound response factors and relative standard deviation for pesticide analysis methods.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055927
Second set of calibration verification data for pesticide analysis of sample AD27626 with recovery and detection limits.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057173
Lab quality control analysis verifying accuracy of pesticide detection methods for sample AD27546.
1 shared topics · Same agency, volume and box · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089991
Raw chromatographic data and compound identification logs for pesticide analysis conducted in December 2001.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089541
Gas chromatography report showing concentrations of multiple pesticides including endrin and heptachlor for sample 508.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089831
Technical report displaying calibration data and relative standard deviations for pesticide analysis methods in early 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000092394
Technical document presenting method validation statistics including average response and relative standard deviation for pesticide analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089527
Instrumental analysis report for a reference pesticide sample from December 26, 2001, documenting compound identification and recovery percentages.
1 shared topics · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089724
Laboratory report detailing specific pesticide concentrations including Endrin and DDT in environmental sample AD28320 analyzed in late 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089583
Duplicate calibration verification results for pesticides and PCBs confirming analytical system performance.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000090012
Laboratory report containing pesticide concentration data and statistical summaries for samples analyzed in December 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089971
Laboratory report listing pesticide concentrations for sample AD27116 analyzed between November 13 and December 7, 2001.
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NYC-WTC_000057144
Inspection log or form for site 508 X covering dates in mid-November and mid-December 2001.
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Index or cover sheet for PCB analysis files covering the period from November 15 to December 13, 2001.
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Laboratory report containing quality control metrics for PCB analysis sample AD27546.
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Laboratory report listing quantitative results for PCBs in sample AD27546.
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NYC-WTC_000057164
Lab quality control analysis verifying accuracy of pesticide detection methods for sample AD27546.
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