Second set of calibration verification data for pesticide analysis of sample AD27626 with recovery and detection limits.
NYC-WTC_000055927–000055933Folder label: “508 X 11/16/01 A 12/14/01 - 12/16/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Signal #1 : C:\MSDCHEM\1\DATA\5O8\O11214C\PESTC2.D\ECD1A.CH Vial: 14 Signal #2 : C:\MSDCHEM\l\DATA\508\011214C\PESTC2.D\ECD2B.CH Acq On : 14 Dec 2001 8:32 pm Operator: Nefliu Sample : pest ic2 Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 27 14:58:19 2001 Quant Results File: 011214P.RES
Quant Method : C:\MSDCHEM\1\METHODS\011214P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 17 10:51:26 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M
Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :
Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1
System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.34 14.97 676.7E6 551.2E6 0.217m 0.196m Spiked Amount 0.200 Recovery = 108.50% 98.00%
Target Compounds 1) Propachlor 9.04 8.49 88164438 75190661 0.184m 0.201m 2) g-BHC 9.82 10.17 2145.6E6 1733.8E6 0.283m 0.285m 3) Heptachlor 10.98 11.22 668.2E6 453.7E6 0.096m 0.095m 4) Aldrin 11.69 11.97 917.9E6 758.1E6 0.121m 0.122m 5) Heptachlor Epoxi 13.13 13.33 1577.OE6 1285.9E6 0.238m 0.239m 6) 4,4-DDE 13.96 14.54 2535.5E6 2081.2E6 0.401m 0.402m 7) Dieldrin 14.54 14.80 542.8E6 445.7E6 0.076m 0.078m 8) Endrin 15.04 15.46 983.4E6 799.3E6 0.197m 0.201m 9) Methoxychlor 16.99 18.01 930.4E6 556.3E6 0.388m 0.394m
(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTC2.D 011214P.M Thu Jan 03 09:43:08 2002 Page 1
NYC-WTC_000055928
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NYC-WTC_000056440
Technical document displaying compound response factors and relative standard deviation for pesticide analysis methods.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057180
Calibration data for pesticide analysis using method 508, showing compound response factors.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055871
Laboratory report listing concentrations of pesticides including Propachlor and Toxaphene in sample AD27776 analyzed via Method 508.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089541
Gas chromatography report showing concentrations of multiple pesticides including endrin and heptachlor for sample 508.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089991
Raw chromatographic data and compound identification logs for pesticide analysis conducted in December 2001.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089831
Technical report displaying calibration data and relative standard deviations for pesticide analysis methods in early 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000092394
Technical document presenting method validation statistics including average response and relative standard deviation for pesticide analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089527
Instrumental analysis report for a reference pesticide sample from December 26, 2001, documenting compound identification and recovery percentages.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089724
Laboratory report detailing specific pesticide concentrations including Endrin and DDT in environmental sample AD28320 analyzed in late 2001.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089583
Duplicate calibration verification results for pesticides and PCBs confirming analytical system performance.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000090012
Laboratory report containing pesticide concentration data and statistical summaries for samples analyzed in December 2001.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089971
Laboratory report listing pesticide concentrations for sample AD27116 analyzed between November 13 and December 7, 2001.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000055890
Inspection log or form for site 508 X covering dates in mid-November and mid-December 2001.
Filed in the same folder
NYC-WTC_000055891
Fragmented document page from a DEP environmental monitoring log covering the period of November to December 2001.
Filed in the same folder
NYC-WTC_000055893
Record of laboratory sample extraction and processing parameters including drip rates and pH levels for samples in late 2001.
Filed in the same folder
NYC-WTC_000055895
Computer-generated sequence file listing analytical samples and methods for pesticide testing conducted in December 2001.
Filed in the same folder
NYC-WTC_000055897
Technical log recording instrument status and data acquisition parameters for environmental sample analysis in late 2001.
Filed in the same folder