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GC/MS analytical results for reference pesticide sample, Dec 2001

Machine-extracted title · confidence 95%

Instrumental analysis report for a reference pesticide sample from December 26, 2001, documenting compound identification and recovery percentages.

NYC-WTC_000089527–000089528

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) r I/, Signal #1 : C:\MSDCHEM\l\DATA\508\011226\1226REFP.D\ECDlA.CH Vial: 67 Signal #2 : C:\MSDCHEM\l\DATA\508\011226\1226REFP.D\ECD2B.CH Acq On : 27 Dec 2001 6:18 am Operator: Nefliu Sample : 12/26 ref pest Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 13:59:07 2001 Quant Results File: 011224P.RES Quant Method : C:\MSDCHEM\1\METHODS\011224P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 10:35:07 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 438.8E6 338.0E6 0.113m 0.116 Spiked Amount 0.200 Recovery 56.50% 58.00%

Target Compounds 1) Propachlor 9.06 8.50 146.5E6 112.6E6 0.279 0.299 2) g-BHC 9.83 10.19 1940.0E6 1484.7E6 0.223 0.241 3) Heptachlor 11.00 11.24 922.1E6 590.5E6 0.115 0.126 4) Aldrin 11.71 11.99 369.4E6 284.1E6 0.042 0.044 5) Heptachlor Epoxi 13.15 13.34 1711.9E6 1314.5E6 0.226 0.238 6) 4,4-DDE 13.98 14.55 3937.8E6 3116.7E6 0.557 0.592 7) Dieldrin 14.56 14.82 961.9E6 727.7E6 0.119 0.123 8) Endrin 15.06 15.47 974.8E6 725.7E6 0.165 0.175 9) Methoxychlor 17.00 18.02 776.3E6 533.7E6 0.322 0.387

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1226REFP.D 011224P.M Mon Dec 31 13:59:35 2001 Page 1

NYC-WTC_000089527

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NYC-WTC_000089527Source: NYC Law Department, mirrored locally

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