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GC/MS analytical results for reextracted sample 27142D, Dec 2001

Machine-extracted title · confidence 95%

Instrumental analysis report for a reextracted sample from December 27, 2001, documenting compound identification and recovery percentages.

NYC-WTC_000089529–000089530

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) ■

Signal #1 : C:\MSDCHEM\l\DATA\508\011226\27142D.D\ECDlA.CH Vial: 68 Signal #2 : C:\MSDCHEM\l\DATA\508\011226\27142D.D\ECD2B.CH Acq On : 27 Dec 2001 6:46 am Operator: Nefliu Sample : 27142 reextracted Inst Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 11:20:12 2001 Quant Results File: 011224P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011224P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 10:35:07 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 411.0E6 297.3E6 0.106m 0.102m Spiked Amount 0.200 Recovery = 53.00% 51.00% Target Compounds 9) Methoxychlor 0.00 18.01 0 20371713 N.D. d 0.015m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 27142D.D 011224P.M Mon Dec 31 11:37:34 2001 Page 1

NYC-WTC_000089529

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NYC-WTC_000089529Source: NYC Law Department, mirrored locally

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