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Pesticide residue analysis, Sample AD28320, Nov-Dec 2001

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Laboratory analysis report for pesticide residues in sample AD28320, showing multiple compounds detected including propachlor, lindane, heptachlor, aldrin, DDE, dieldrin, endrin…

NYC-WTC_000089753–000089756

Folder label: “508 X 11/28/01 A 12/24-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011224B\1128REFP.D\ECDlA.CH Vial: 21 Signal #2 : C:\MSDCHEM\l\DATA\508\011224B\1128REFP.D\ECD2B.CH Acq On : 24 Dec 2001 10:14 pm Operator: Nefliu Sample : 11/28 ref pest Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 12:24:23 2001 Quant Results File: 011224P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011224P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 10:35:07 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 731.3E6 527.4E6 0.188m 0.180m Spiked Amount 0.200 Recovery 94.00% 90.00% Target Compounds 1) Propachlor 9.06 8.50 151.8E6 116.3E6 0.289 0.309 2) g-BHC 9.83 10.18 2158.9E6 1568.1E6 0.248 0.254 3) Heptachlor 11.00 11.23 993.1E6 582.6E6 0.124 0.124 4) Aldrin 11.70 11.98 398.8E6 293.5E6 0.046m 0.046 5) Heptachlor Epoxi 13.14 13.34 1891.4E6 1416.9E6 0.250 0.257 6) 4,4-DDE 13.97 14.55 4424.0E6 3359.4E6 0.626 0.638 7) Dieldrin 14.55 14.81 1081.6E6 792.2E6 0.134 0.133 8) Endrin 15.06 15.47 1117.7E6 783.9E6 0.190 0.189 9) Methoxychlor 17.00 18.02 920.1E6 572.1E6 0.382m 0.415m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1128REFP.D 011224P.M Mon Dec 31 13:51:10 2001 Page 1

NYC-WTC_000089755

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NYC-WTC_000089755Source: NYC Law Department, mirrored locally

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