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← Document results/DEP Box 68/508 X 1/7/02 A 1/10-1/11/02
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Pesticide method validation data, Jan 2002

Machine-extracted title · confidence 100%

Technical report displaying calibration data and relative standard deviations for pesticide analysis methods in early 2002.

NYC-WTC_000089831–000089837

Folder label: “508 X 1/7/02 A 1/10-1/11/02

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NYC 9/11 Public Portal Document

/ • Response Factor Report Instrumen

Method : C:\MSDCHEM\1\METHODS\020110P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Jan 11 09:04:07 2002

Calibration Files 1 =PESTC1.D 2 =PESTC2.D 3 =PESTC3.D

Compound 1 2 3 Avg %RSD

1) Propachlor 6.231 4.946 4.422 5.200 E8 17.90 2) ■■ g-BHC 8.032 7.986 7.786 7.934 E9 1.65 3) Heptachlor 7.096 7.205 7.247 7.183 E9 1.09 4) Aldrin 8.083 8.087 7.884 8.018 E9 1.45 5) Heptachlor Epoxide 7.351 6.967 6.646 6-. 988 E9 5.05 6) 4,4-DDE 5.973 6.168 5.993 6.045 E9 1.78 7) Dieldrin 6.202 6.949 6.888 6.680 E9 6.21 8) Endrin 4.555 4.692 4.681 4.643 E9 1.64 9) Methoxychlor 1.857 2.176 1.974 2.002 E9 8.08 10) S 2,4-DDD SURROGATE 3.386 3.690 3.886 3.654 E9 6.90

Signal #2 Calibration Files 1 =PESTC1.D 2 =PESTC2.D 3 =PESTC3.D

Compound 1 2 3 Avg %RSD

1) Propachlor 4.397 3.987 3.632 4.005 E8 9.56 2) g-BHC 6.373 6.581 6.484 6.479 E9 1.6 0 3) Heptachlor 5.128 5.194 5.296 5.206 E9 1.63 4) Aldrin 6.453 6.683 6.571 6.569 E9 1.75 5) Heptachlor Epoxide 5.801 5.710 5.503 5.671 E9 2.69 6) 4,4-DDE 4.855 5.054 4.929 4.946 E9 2.04 7) Dieldrin 6.632 6.833 6.618 6.694 E9 1.80 8) Endrin 3.528 3.795 3.817 3.714 E9 4.33 9) Methoxychlor 1.195 1.409 1.397 1.333 E9 9.02 10) s 2,4-DDD SURROGATE 3.026 3.307 3.425 ' 3.253 E9 6.30

(#) = Out of Range 020110P.M Fri Jan 11 10:23:06 2002 Page 1

NYC-WTC_000089831

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NYC-WTC_000089831Source: NYC Law Department, mirrored locally

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