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Sample AD28167 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28167 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055481–000055486

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\012502A\28167RR.D Vial: 8 . Acq On : 25 Jan 2002 7:55 pm Operator: McLean Sample : REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:44:07 2002 Quant Results File: 012402B.RES

Quant Method Title Last Update Response via DataAcq Meth : : : : : C:\MSDCHEM\l\5973N\012402B.M (RTE Integrator) Quantitation For Method 525.2 Fri Jan 25 11:19:14 2002 Initial Calibration 012402DF AeuloAn Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 15578538 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 19075988 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 14028863 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 4142674 5.19 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.80% 19) Triphenyl Phosphate 29.33 326 3420897 5.95 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.00% 21) Perylene D-12 34.02 264 8149808 4.09 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.13 284 26451 0.03 ug/L 92 5) EPTC 15.83 128 5581 Below Cal # 1 6) 2,6-Dinitrotoluene 17.52 165 9878 0.83 ug/L 82 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 18.91 126 20080 Below Cal # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 . 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.68 162 6950 0.22 ug/L 38 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.05 246 8924 0.04 ug/L 67 22) Bis (2-Ethylhexyl) adipate 29.26 129 56854 0.53 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.69 149 642517 0.60 ug/L 95 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28167RR.D 012402B.M Mon Jan 28 12:45:32 2002 Page 1

NYC-WTC_000055484

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NYC-WTC_000055484Source: NYC Law Department, mirrored locally

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