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← Document results/DEP Box 30/525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02
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Sample AD28049 Method 525.2 analysis, Jan 2002

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Laboratory results for sample AD28049 analyzing pesticides and organic contaminants using Method 525.2.

NYC-WTC_000055451–000055456

Folder label: “525 X 11/21/01 A 12/11/01 + REANALYSIS 1/25/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\012502A\28049RR.D Vial: 23 Acq On : 26 Jan 2002 7:10 am Operator: McLean Sample : REINJ Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:23:55 2002 Quant Results File: 012402B.RES . A

Quant Method Title Last Update Response via DataAcq Meth : : : : : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Quantitation For Method 525.2 Fri Jan 25 11:19:14 2002 Initial Calibration 012402DF /oyktoo Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 17.96 164 14023784 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 18972084 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 14998220 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3602609 5.01 ug/L 0.00 Spiked Amount 5,000 Recovery = 100.20% 19) Triphenyl Phosphate 29.32 326 3623957 6.34 ug/L 0.00 Spiked Amount 5.000 Recovery = 126.80% 21) Perylene D-12 34.02 2.64 9278876 4.36 ug/L 0.00 Spiked Amount 5.000 Recovery = 87.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 15.83 128 7429 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.71 165 16657 0.92 ug/L 38 8) Molinate 18.91 126 7286 Below Cal # 1 10) Simazine 21.47 201 5828 0.52 ug/L # 18 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 23.30 160 8330 0.15 ug/L # 15 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. d 15) Metribuzin 0.00 198 0 N.D. d 16) Metolachlor 0.00 162 0 N.D. d 17) Butachlor 26.38 160 110265 0.48 ug/L 92 18) 4,4'-DDE 27.06 246 6543 0.04 ug/L 63 22) Bis (2-Ethylhexyl) adipate 29.25 129 46475 0.52 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.69 149 335198 0.48 ug/L 91 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28049RR.D 012402B.M Mon Jan 28 12:24:53 2002 Page 1

NYC-WTC_000055454

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NYC-WTC_000055454Source: NYC Law Department, mirrored locally

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