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Sample analysis results, sample AD27546, Dec 2001

Machine-extracted title · confidence 90%

Primary sample analysis for AD27546 testing pesticides and organic compounds with most results below detection limits.

NYC-WTC_000055166–000055169

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Dta • ile C:\MSDCHEM\l\DATA\120601\27546.D Vial: 19 ■ Acq On 7 Dec 2001 6:10 am Operator: McLean Sample 11/19 sample Inst : Instrumen Mise Multiple: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 07 06:47:48 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.31 164 6130993 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 10234651 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 6757202 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1338288 4.11 ug/L 0.00 Spiked Amount 5.000 Recovery = 82.20% 19) Triphenyl Phosphate surr 29.69 326 2035624 5.74 ug/L 0.00 Spiked Amount 5.000 Recovery = 114.80% 21) Perylene D-12 surr 34.44 264 4169729 4.40 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.81 237 5224 0.03 ug/L 85 4) Hexachlorobenzene 21.51 284 19721 0.04 ug/L # 74 5) EPTC 16.28 128 5131 0.01 ug/L # 1 6) 2,6-Dinitrotoluene 17.93 165 185252 1.00 ug/L # 35 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.22 126 12859 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.95 162 13995 0.01 ug/L 78 17) Butachlor 26.76 160 49241 0.12 ug/L # 9 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 27781 0.14 ug/L # 27 23) Bis (2-Ethylhexyl) phthala 31.07 149 1258721 0.89 ug/L 97 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27546.D 5080102.M Thu Jan 10 08:48:27 2002 Page 1

NYC-WTC_000055167

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NYC-WTC_000055167Source: NYC Law Department, mirrored locally

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