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Lab blank results, sample AD27491, Dec 2001

Machine-extracted title · confidence 90%

Laboratory blank analysis for sample AD27491 showing non-detect levels for pesticides and organic compounds.

NYC-WTC_000055140–000055142

Folder label: “525 X 11/19/01 A 12/6/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\lll9LB.D Vial: 8 Acq On 6 Dec 2001 9:15 pm Operator: McLean Sample lb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 06 21:52:46 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.32 164 4526595 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 8071121 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 5181540 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 954917 3.97 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.40% 19) Triphenyl Phosphate surr 29.70 326 1381912 4.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.80% 21) Perylene D-12 surr 34.45 264 3213658 4.42 ug/L 0.00 Spiked Amount 5.000 Recovery = 88.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 17.93 165 21010 0.35 ug/L # 47 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.09 126 5102 0.01 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 26.76 160 36238 0.11 ug/L # 1 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 10794 0.12 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 320331 0.41 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 1119LB.D 5080102.M Thu Jan 10 08:56:47 2002 Page 1

NYC-WTC_000055141

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NYC-WTC_000055141Source: NYC Law Department, mirrored locally

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