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ICPMS daily performance check report, May 21, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 21, 2002.

NYC-WTC_000053939–000054155

Folder label: “ICPMS 5/21/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10603 Sample Date/Time: Tuesday, May 21, 2002 11:36:01 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE1 0603.215 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 16968.000 3.126 0.379 52.76500 3.54 ug/L Li 6 44723.522 0.513 44723.522 ug/L > Se-1 45 353323.994 1.755 353323.994 ug/L Cr 52 377408.420 2.013 1.053 49.68426 2.52 ug/L Cr 53 45174.084 0.930 0.126 49.80511 2.71 ug/L Mn 55 933641.509 1.129 2.640 74.18675 2.66 ug/L Co 59 452798.260 1.237 1.282 49.52777 2.96 ug/L Ni 60 93565.320 0.895 0.265 49.31484 2.57 ug/L Cu 63 214253.530 2.122 0.606 50.92967 3.37 ug/L Cu 65 105125.874 2.003 0.297 50.81645 3.78 ug/L Zn 66 74461.187 1.952 0.877 53.10487 2.50 ug/L Zn 67 13068.518 1.478 0.154 52.05410 0.41 ug/L Zn 68 55961.272 0.263 0.660 53.65386 1.46 ug/L Ge 72 84129.367 1.341 84129.367 ug/L As 75 102588.376 1.287 1.084 53.20762 0.78 ug/L Se 77 10285.153 2.148 0.105 55.70171 0.96 ug/L Se 82 10305.468 1.312 0.124 54.89778 0.65 ug/L As-1 75 86366.200 1.029 86203.530 47.85564 1.03 ug/L Kr 83 4522.170 1.363 -249.130 ug/L Ag 107 451790.305 1.518 0.379 46.88755 2.08 ug/L Cd 111 124127.940 0.701 0.104 50.45226 1.10 ug/L Cd 114 290162.998 1.195 0.243 50.42086 1.04 ug/L In 115 1192476.711 0.599 1192476.711 ug/L Sb 121 423606.473 0.775 0.355 52.30618 0.56 ug/L Sb 123 326582.492 1.320 0.274 52.61669 0.92 ug/L Ba 135 158210.862 1.291 0.088 67.65597 0.78 ug/L Ba 137 278990.451 1.682 0.155 68.52993 0.96 ug/L Ho 165 1844692.658 1.791 0.007 ug/L > Tb 159 1803294.412 0.722 1803294.412 ug/L Hg 201 5633.135 1.590 0.003 4.24568 1.49 ug/L Hg 202 12760.746 1.694 0.007 4.17648 1.02 ug/L TI 205 1394719.255 2.034 0.773 49.58098 1.82 ug/L Pb 208 1889986.453 1.059 1.047 49.18486 0.82 ug/L

Sample ID: AE10603 Report Date/Time: Tuesday, May 21, 2002 11:47:30 Page 1

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