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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09683 Sample Date/Time: Thursday, May 16, 2002 10:44:19 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09683.139 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 18653.312 2.576 0.365 51.76313 3.24 ug/L LI 6 51144.035 2.604 51144.035 ug/L > Sc-1 45 401786.497 1.938 401786.497 ug/L Cr 52 436176.143 1.411 1.071 50.35654 2.58 ug/L Cr 53 53657.421 0.043 0.132 52.13913 2.00 ug/L Mn 55 1427337.748 0.769 3.549 99.87829 1.38 ug/L Co 59 513106.755 1.318 1.277 49.78313 1.77 ug/L Ni 60 111487.174 2.511 0.277 52.65697 0.62 ug/L Cu 63 258237.999 1.736 0.642 55.79616 1.53 ug/L Cu 65 125150.280 1.635 0.311 55.15535 1.47 ug/L Zn 66 81752.477 1.460 0.883 51.39473 1.10 ug/L Zn 67 14445.614 1.469 0.156 51.43919 1.14 ug/L Zn 68 62177.261 2.220 0.671 52.61528 1.07 ug/L > Ge 72 91761.840 2.146 91761.840 ug/L As 75 106000.543 2.702 1.105 53.36459 2.03 ug/L Se 77 10540.604 0.118 0.108 55.70112 2.22 ug/L Se 82 11872.679 1.653 0.130 56.57180 3.50 ug/L As-1 75 96696.497 3.114 96498.493 47.06552 3.12 ug/L Kr 83 1968.233 1.365 -60.681 ug/L Ag 107 450241.463 3.758 0.359 43.59997 4.19 ug/L Cd 111 131090.487 1.425 0.105 50.11529 0.55 ug/L Cd 114 305962.609 2.286 0.244 49.99635 1.42 ug/L > In 115 1252915.467 1.460 1252915.467 ug/L Sb 121 453380.475 1.680 0.362 53.52739 0.94 ug/L Sb 123 346242.672 0.918 0.276 53.28880 0.76 ug/L Ba 135 202822.373 2.339 0.108 76.15339 0.36 ug/L Ba 137 357803.567 1.733 0.190 77.00836 1.51 ug/L Ho 165 1881899.777 1.905 -0.018 ug/L > Tb 159 1886163.008 2.596 1886163.008 ug/L Hg 201 5601.115 1.617 0.003 3.81855 1.06 ug/L Hg 202 12479.686 1.327 0.007 3.73826 1.36 ug/L TI 205 1399845.117 2.054 0.742 45.76072 2.34 ug/L Pb 208 1915404.754 1.534 1.015 46.15250 1.05 ug/L

Sample ID: AE09683 Report Date/Time: Thursday, May 16, 2002 10:46:59 Page 1

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