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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09683 Sample Date/Time: Thursday, May 16, 2002 10:14:56 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09683.137 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 18820.985 0.770 0.367 52.03716 1.46 ug/L Li 6 51319.639 1.250 51319.639 ug/L > Se-1 45 413017.172 1.745 413017.172 ug/L Cr 52 449800.684 2.684 1.074 50.50167 1.37 ug/L Cr 53 54422.984 1.530 0.130 51.42396 0.52 ug/L Mn 55 1468033.902 1.817 3.551 99.91510 0.07 ug/L Co 59 518287.996 1.437 1.255 48.92382 2.77 ug/L Ni 60 116010.348 2.661 0.281 53.31449 2.86 ug/L Cu 63 261310.031 1.350 0.632 54.92615 1.73 ug/L Cu 65 124973.071 2.519 0.302 53.58614 3.32 ug/L Zn 66 82467.883 1.133 0.886 51.59002 2.23 ug/L Zn 67 14742.428 2.166 0.158 52.23363 1.43 ug/L Zn 68 61987.633 2.154 0.666 52.18217 0.19 ug/L > Ge 72 92232.245 2.201 92232.245 ug/L As 75 107245.312 1.155 1.113 53.73805 1.08 ug/L Se 77 11003.468 0.993 0.112 57.98562 1.91 ug/L Se 82 11929.773 0.401 0.130 56.54310 1.88 ug/L As-1 75 98641.665 1.493 98443.661 48.01425 1.50 ug/L Kr 83 1967.233 3.926 -61.681 ug/L Ag 107 439152.708 1.154 0.351 42.59237 0.48 ug/L Cd 111 132695.651 1.933 0.106 50.82123 1.98 ug/L Cd 114 307550.934 0.744 0.246 50.34855 0.23 ug/L > In 115 1250670.756 0.846 1250670.756 ug/L Sb 121 450752.800 0.633 0.360 53.31576 1.28 ug/L Sb 123 346959.623 0.964 0.277 53.49205 0.65 ug/L Ba 135 203712.775 1.372 0.109 77.10882 1.60 ug/L Ba 137 355429.559 1.612 0.190 77.10100 1.02 ug/L Ho 165 1891637.566 1.564 -0.005 ug/L > Tb 159 1871300.228 2.445 1871300.228 ug/L Hg 201 6326.598 2.178 0.003 4.35128 1.88 ug/L Hg 202 14123.104 1.181 0.008 4.26763 1.63 ug/L n 205 1388668.582 1.637 0.742 45.75703 2.31 ug/L Pb 208 1922734.376 1.474 1.027 46.69684 1.08 ug/L

Sample ID: AE09683 Report Date/Time: Thursday, May 16, 2002 10:17:15 Page 1

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