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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: Blank Sample Date/Time: Tuesday, May 14, 2002 09:01:47 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\Blank.OO1 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 10.333 33.986 ug/L > Se-1 45 704701.937 1.435 ug/L Cr 52 10613.632 0.746 ug/L Cr 53 1017.734 4.312 ug/L Mn 55 1379.452 5.053 ug/L Ni 60 44.334 14.502 ug/L Cu 63 386.679 6.912 ug/L Cu 65 194.337 5.206 ug/L Zn 66 1144.417 8.152 ug/L Zn 67 216.338 8.389 ug/L Zn > Ge As Se 68 72 75 77 874.718 144456.865 6440.884 944.792 12.663 1.059 1.713 1.255 CF 2%/ Reviewed, by, ug/L ug/L ug/L ug/L Se 82 -16.113 698.877 ug/L Kr 83 2504.704 4.085 ug/L Ag 107 370.011 8.059 ug/L > In 115 1863580.239 0.458 ug/L Sb 121 35.334 13.375 ug/L Sb 123 34.019 41.267 ug/L Ba 135 54.667 30.463 ug/L Ba 137 94.668 6.367 ug/L > Tb 159 2688035.637 0.326 ug/L Hg 201 46.334 10.647 ug/L Hg 202 96.001 7.217 ug/L TI 205 957.393 6.794 ug/L Pb 208 2938.215 2.264 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Se-1 45 Cr 52 Cr 53 Mn 55

Sample ID: Blank Report Date/Time: Tuesday, May 14, 2002 09:03:28 Page 1

NYC-WTC_000053390

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NYC-WTC_000053390Source: NYC Law Department, mirrored locally

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