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ICPMS daily performance check report, April 25, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on April 25, 2002.

NYC-WTC_000053337–000053387

Folder label: “ICPMS 4/25/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: Blank Sample Date/Time: Thursday, April 25, 2002 14:12:34 Sample Type: Sample Sample Description: V t pKEAY1, Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth —T Dataset File: c:\winnt\profiles\lrd1\elandata\dataset\newyork cit\Blank.689 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.333 18.330 ug/L Sc-1 45 419344.601 0.467 ug/L Cr 52 6445.015 1.274 ug/L Cr 53 480.351 0.731 ug/L Mn 55 1465.800 2.426 ug/L Ni 60 145.336 4.581 ug/L Cu 63 306.675 2.959 ug/L Cu 65 168.337 3.272 ug/L Zn 66 852.715 3.014 ug/L Zn 67 157.336 12.622 ug/L Zn 68 673.032 4.385 ug/L > Ge 72 82199.167 1.679 ug/L As 75 118.781 46.707 ug/L Se 77 94.919 12.675 ug/L Se 82 101.668 7.250 ug/L Ag 107 105.668 5.381 ug/L In 115 1183093.732 1.401 ug/L Sb 121 23.334 36.450 ug/L Sb 123 21.861 7.306 ug/L Ba 135 37.667 5.527 ug/L Ba 137 48.334 7.833 ug/L Ho 165 1639168.252 1.000 ug/L Tb 159 1658083.017 1.643 ug/L Hg 201 42.667 33.173 ug/L Hg 202 72.334 11.175 ug/L Tl 205 1001.399 7.447 ug/L Pb 208 1793.755 0.170 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 Cr 52 Cr 53 Mn 55

Sample ID: Blank Report Date/Time: Thursday, April 25, 2002 14:14:15 Page 1

NYC-WTC_000053338

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NYC-WTC_000053338Source: NYC Law Department, mirrored locally

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