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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10067 Sample Date/Time: Tuesday, May 14, 2002 13:14:14 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1 \elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE10067.053 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean. Gone. Mean Cone. RSD Sample Unit Be 9 12.333 23.406 0.000 0.01120 59.95 ug/L Sc-1 45 516536.653 0.367 516536.653 ug/L Cr 52 11704.983 2.285 0.008 0.35553 7.18 ug/L Cr 53 2781.787 1.299 0.004 1.55323 1.31 ug/L Mn 55 466589.087 0.947 0.901 25.11460 1.18 ug/L Ni 60 1300.106 0.887 0.002 0.46322 0.81 ug/L Cu 63 58999.133 1.950 0.114 10.05691 2.30 ug/L Cu 65 27924.107 1.608 0.054 9.94184 1.82 ug/L Zn 66 21040.198 0.924 0.184 10.84332 0.95 ug/L Zn 67 3370.659 3.108 0.029 9.81416 1.80 ug/L Zn 68 15934.780 0.688 0.139 11.00771 1.96 ug/L > Ge 72 109641.384 1.437 109641.384 ug/L As 75 6234.806 0.480 0.012 0.59907 4.62 ug/L Se 77 941.833 2.591 0.002 1.07727 9.70 ug/L Se 82 85.800 97.197 0.001 0.39786 85.04 ug/L Kr 83 2134.272 3.596 -370.432 ug/L Ag 107 99.002 4.040 -0.000 -0.01530 2.01 ug/L > in 115 1475344.343 0.896 1475344.343 ug/L Sb 121 380.012 2.248 0.000 0.03860 1.49 ug/L Sb 123 270.280 7.295 0.000 0.03510 8.14 ug/L Ba 135 29048.962 0.762 0.012 8.99447 0.93 ug/L Ba 137 50725.976 0.943 0.020 8.93086 1.38 ug/L > Tb 159 2506921.621 0.750 2506921.621 ug/L Hg 201 57.334 6.125 0.000 0.00904 23.09 ug/L Hg 202 114.335 20.997 0.000 0.00699 99.41 ug/L TI 205 962.727 6.578 0.000 0.00185 83.49 ug/L Pb 208 14142.767 0.707 0.005 0.24379 0.41 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 > Sc-1 45 73.299 Cr 52 Cr 53 Mn 55

Sample ID: AE10067 Report Date/Time: Tuesday, May 14, 2002 13:15:55 Page 1

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