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ICPMS daily performance check report, May 9, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 9, 2002.

NYC-WTC_000053212–000053335

Folder label: “ICPMS 5/9/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09395 Sample Date/Time: Thursday, May 09,2002 10:42:02 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE09395.850 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 12.667 9.116 0.000' 0.00370 77.35 ug/L Li 6 56379.889 1.847 56379.889 mg/L Se-1 45 489023.745 1.993 489023.745 ug/L Cr 52 11587.163 1.621 0.009 0.42389 5.79 ug/L Cr 53 2141.607 2.143 0.003 1.01416 0.47 ug/L Mn 55 262953.954 1.077 0.532 14.46514 1.15 ug/L Ni 60 1015.067 1.880 0.002 0.34335 3.81 ug/L Cu 63 8724.272 1.598 0.017 1.34486 1.04 ug/L Cu 65 4200.012 0.104 0.008 1.29740 1.96 ug/L Zn 66 4276.048 2.083 0.009 0.56002 2.43 ug/L Zn 67 948.726 2:742 0.003 1.15069 3.13 ug/L Zn 68 3782.158 1.362 0.011 0.88321 7.17 ug/L Ge 72 122012.319 1.451 122012.319 ug/L As 75 10969.492 1.587 0.005 0.23038 26.82 ug/L Se 77 1393.284 1.699 0,000 0.07594 190.86 ug/L Se 82 -178.794 52.597 -0.001 -0.36198 89.87 ug/L As-1 75 1024.068 2.912 780.729 0.30618 3.82 ug/L Kr 83 4070.286 3.096 -323.487 ug/L Ag 107 227.338 14.086 0.000 0.00429 54.23 ug/L Cd 111 149.003 5.242 0.000 0.01432 17.65 ug/L Cd 114 322.733 12.830 0.000 0.01505 34.58 ug/L In 115 1730480.314 1.143 1730480.314 ug/L Sb 121 675.699 4.672 0.000 0.05347 3.85 ug/L Sb 123 515.785 5.216 0.000 0.05277 4.81 ug/L Ba 135 54444.100 1.171 0.020 14.92060 1.42 ug/L Ba 137 94108.534 0.331 0.035 14.80682 0.29 ug/L Ho 165 2753649.651 0.537 0.002 ug/L > Tb 159 2696996.662 0.361 2696996.662 ug/L Hg 201 81.335 12.619 0,000 0.01113 49.89 ug/L Hg 202 173.670 9.468 0.000 0.01298 30.11 ug/L TI 205 747.038 7.186 -0.000 -0.00933 13.06 ug/L Pb 208 7341.882 2.667 0.002 0.08070 3.93 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff

Sample ID: AE09395 Report Date/Time: Thursday, May 09, 2002 10:43:56 Page 1

NYC-WTC_000053258

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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