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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09333 Sample Date/Time: Wednesday, May 08, 2002 13:05:52 Sample Type: Spike - 1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09333.804 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 20108.418 1.310 0.046' 57.45152 0.64 ug/L Se-1 45 439475.707 1.939 439475.707 ug/L Cr 52 487941.234 1.263 1.095 49.91203 2.80 ug/L Cr 53 59074.007 2.862 0.133 50.41085 1.61 ug/L Mn 55 1317536.526 2.516 2.985 81.29348 2.92 ug/L Ni 60 139287.175 1.645 0.317 54.01004 3.11 ug/L Cu 63 335370.196 0.798 0.763 58.06715 2.20 ug/L Cu 65 167075.241 1.698 0.380 58.90305 3.14 ug/L Zn 66 106108.732 0.730 0.899 54.15087 1.01 ug/L Zn 67 18609.881 0.509 0.157 52.48169 1.26 ug/L Zn 68 80852.170 1.886 0.684 54.29028 0.94 ug/L > Ge 72 117290.003 1.054 117290.003 ug/L As 75 137936.609 0.564 1.086 52.44921 0.56 ug/L Se 77 13781.674 1.422 0.106 56.18981 0.49 ug/L Se 82 14741.892 0.640 0.126 55.92397 1.59 ug/L Kr 83 4041.939 0.220 -419.534 ug/L Ag 107 620432.253 0.904 0.365 42.74959 1.64 ug/L In 115 1700287.288 1.195 1700287.288 ug/L Sb 121 599846.365 1.085 0.353 51.55962 0.30 ug/L Sb 123 461674.588 1.230 0.271 51.90608 0.22 ug/L Ba 135 232765.148 1.261 0.090 61.50476 0.78 ug/L Ba 137 408446.738 1.152 0.158 61.63037 0.68 ug/L Tb 159 2578925.975 0.479 2578925.975 ug/L Hg 201 7538.534 1.696 0.003 4.20872 1.28 ug/L Hg 202 16915.561 1.523 0.006 4.18445 1.34 ug/L n 205 1797023.581 0.940 0.696 45.44836 0.70 ug/L Pb 208 2501709.070 0.892 0.969 47.63566 0.59 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 114.859 Se-1 45 85.942 Cr 52 99.578 Cr 53 99.500 Mn 55 101.871

Sample ID: AE09333 Report Date/Time: Wednesday, May 08, 2002 13:08:17 Page 1

NYC-WTC_000053151

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