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ICPMS daily performance check report, May 8, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09151 Sample Date/Time: Wednesday, May 08, 2002 11:22:48 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09151.788 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 20521.677 1.233 0.043' 53.86878 0.95 ug/L > Se-1 45 478346.141 2.152 478346.141 ug/L Cr 52 507301.268 1.534 1.045 47.63461 1.51 ug/L Cr 53 61733.578 2.177 0.127 48.38726 2.52 ug/L Mn 55 1336458.939 1.321 2.781 75.73314 1.58 ug/L Ni 60 148316.477 1.784 0.310 52.82556 1.64 ug/L Cu 63 329390.705 0.817 0.688 52.39767 2.49 ug/L Cu 65 162074.593 0.159 0.339 52.48951 2.31 ug/L Zn 66 112752.767 1.187 0.890 53.59391 1.54 ug/L Zn 67 19753.644 2.415 0.156 51.88519 2.91 ug/L Zn 68 84086.971 1.257 0.663 52.58412 1.30 ug/L > Ge 72 125918.990 0.475 125918.990 ug/L As 75 146268.642 1.333 1.072 51.74982 1.09 ug/L Se 77 14631.456 0.700 0.104 55.49927 1.10 ug/L Se 82 15955.186 1.608 0.127 56.37464 2.07 ug/L Kr 83 4231.027 0.818 -230.446 ug/L Ag 107 706288.986 0.474 0.382 44.75287 0.90 ug/L > in 115 1848868.219 0.887 1848868.219 ug/L Sb 121 639874.083 1.791 0.346 50.57726 1.05 ug/L Sb 123 493318.733 1.099 0.267 51.00617 0.50 ug/L Ba 135 240236.608 0.489 0.088 60.25424 1.09 ug/L Ba 137 419207.404 0.290 0.154 60.04254 1.44 ug/L > Tb 159 2717243.956 1.316 2717243.956 ug/L Hg 201 7338.701 1.151 0.003 3.88395 1.61 ug/L Hg 202 16767.617 0.182 0.006 3.93336 1.22 ug/L TI 205 1888198.362 1.056 0.694 45.32573 0.93 ug/L Pb 208 2519108.711 1.388 0.926 45.52341 0.58 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 107.708 > Sc-1 45 93.544 Cr 52 95.036 Cr 53 96.166 Mn 55 97.998

Sample ID: AE09151 Report Date/Time: Wednesday, May 08, 2002 11:25:05 Page 1

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