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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: Blank Sample Date/Time: Wednesday, May 08,2002 10:30:17 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth \P g Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\Blank.776 \ v Aliquot Volume (mL): Y Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Gone. Mean Cone. RSD Sample Unit Be 9 11.667 19.795 ug/L > Se-1 45 511361.934 2.392 ug/L Cr 52 8144.730 2.517 ug/L Cr 53 853.382 9.914 ug/L Mn 55 7020.448 2.570 ug/L Ni 60 100.668 51.131 ug/L Cu 63 258.340 1.612 ug/L Cu 65 183.670 11.477 jowed by, ug/L Zn Zn 66 67 772.374 176.003 4.931 2.049 /22/20/ ug/L ug/L Zn 68 650.030 7.798 ug/L Ge 72 130722.136 0.648 ug/L As 75 11751.784 0.195 ug/L Se 77 1553.902 0.111 ug/L Se 82 -64.476 21.721 ug/L Kr 83 4461.472 0.561 ug/L Ag 107 425.681 3.241 ug/L > in 115 1906968.925 1.175 ug/L Sb 121 125.002 7.332 ug/L Sb 123 106.936 5.235 ug/L Ba 135 55.667 26.906 ug/L Ba 137 92.001 7.838 ug/L > Tb 159 2676096.668 1.107 ug/L Hg 201 124.335 14.925 ug/L Hg 202 266.007 22.104 ug/L TI 205 1629.829 2.767 ug/L Pb 208 2931.548 2.095 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 Cr 52 Cr 53 Mn 55

Sample ID: Blank Report Date/Time: Wednesday, May 08, 2002 10:31:58 Page 1

NYC-WTC_000053095

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NYC-WTC_000053095Source: NYC Law Department, mirrored locally

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