GCMS analysis results for sample AE01335, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\1335.D Vial: 9 Acq On : 19 Feb 2002 6:11 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Toluene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.47 1.09 ug/1 79542 1,4 -Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Q Toluene 92 C7H8 000108-88-3 91 2 1/375-Cycloheptatriene 92 C7H8 000544-25-2 72 3 Tetracyclo [3.2.0.02,7.04,6] heptane 92 C7H8 000278-06-8 64 4 2,5-Norbornadiene 92 C7H8 000121-46-0 50 Abundance Scan 155 (6.468 min): 1335.D (-) : m/z 91.00 100.00% C1

5000

39 ... 4 65 _ 6.20 6.40 6.60__6.80__ ... n.... ml.. ..p 11 < 11.,, ।,, ,7,,.,. ।, 86 . 1 1 1 11T ।...... . m/z 92.00 64.57% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #63030: Toluene 91

5000 ____ 6.20 6.40 6.60 6.80 m/z 39.05 11.16% 45 51 61 65 Puuumou*uuuammuawDmmmmTIPITWTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance 91

__ 6.20 6.40 6.60 6.80 5000 m/z 64.95 10.65% 65 27 37 46 51 61 ' i " ' ■ i • ■■ ■ r ' ' r ■'' r1'■i■■■■i1■" r ' " i " '' i'' ■ ■ i■'■'i■'11111 " 111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #963: Tetracyclo[3.2.0.02,7.04,6]heptane ......................... 91 _ 6.20 6.40 6-60 6.80__ m/z 62.95 7.01% 5000 66 27 3s 51 11 " ''i'1 r'111 " 11111111 " 11'1 111111111 " I " 11 ' 1 " ■ ■ r ■11111111 " 111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 6.20 6.40 6.60 6.80

1335.D GCMS0208.M Thu Feb 21 15:27:43 2002 Page 1

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