GCMS analysis results for sample AE01405, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01405 conducted on February 27, 2002.

NYC-WTC_000052936–000052943

Folder label: “GCMS X 1/10/02 A 2/19/02”

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Data File : C:\HPCHEM\l\DATA\FEB1902\1405.D Vial: 14 Acq On : 19 Feb 2002 11:01 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 15:08 2002 <Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 290210 20.00 ug/1 -0.02 10) Naphthalene-d8 15.98 136 1111199 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.28 164 571136 20.00 ug/1 -0.03 29) Phenanthrene-dlO 25.73 188 786816 20.00 ug/1 -0.03 38) Chrysene-dl2 33.79 240 497359 20.00 ug/1 -0.05 44) Perylene-dl2 38.08 264 330947 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 34038 4.31 ug/mL 0.31 Spiked Amount 5.000 Recovery = 86.20%

Target Compounds 2) N-nitroso-dimethyl amine 3) bis(2-Chloroethyl)ether 4) 1,3-Dichlorobenzene 5) 1,4-Dichlorobenzene 6) 1,2-Dichlorobenzene 7) 2,2'-oxybis(1-Chloropropan 8) N-Nitroso-di-n-propylamine 9) Hexachloroethane 11) Nitrobenzene 12) Isophorone 13) bis(2-Chloroethoxy)methane 14) 1,2,4-Trichlorobenzene 15) Naphthalene 16) Hexachlorobutadiene 18) Hexachlorocyclopentadiene 19) 2-Chloronaphthalene 20) Dimethylphthalate 21) 2,6-Dinitrotoluene 2 2) Acenaphthylene 23) Acenaphthene 24) 2,4-Dinitrotoluene 25) Diethylphthalate 26) 4-Chlorophenyl-phenylether 27) Fluorene 28) Azobenzen/ 1,2-Diphenylhyd Qvalue 0.00 74 0 N.D. 0.00 93 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 146 0 N.D. 0.00 45 0 N.D. 0.00 70 0 N.D. 0.00 117 0 N.D. 0.00 77 0 N.D. 0.00 82 0 N.D. 0.00 93 0 N.D. 0.00 180 0 N.D. 16.02 128 315 N.D. 0.00 225 0 N.D. 0.00 237 0 N.D. 0.00 162 0 N.D. 0.00 163 0 N.D. 0.00 165 0 N.D. 0.00 152 0 N.D. 0.00 153 0 N.D. 0.00 165 0 N.D. 22.77 149 171 N.D. 0.00 204 0 N.D. 0.00 166 0 N.D. 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1405.D GCMS0208.M Thu Feb 21 15:13:51 2002 Page 1

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