NYC-WTC_000052790
GC/MS blank analysis report for sample AE01041 showing volatile organic compound results generated on February 20, 2002.
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GCMS blank analysis results for sample AE01330, Feb 2002
Machine-extracted title · confidence 100%Laboratory report documenting blank analysis for organic compounds in sample AE01330 to verify analytical system cleanliness on February 21, 2002.
NYC-WTC_000052860–000052867Folder label: “GCMS X 1/10/02 A 2/19/02”
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NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\FEB1902\LB.D Vial: 3 Acq On : 19 Feb 2002 11:13 am Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 12:36 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 260524 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 972411 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.28 164 503822 20.00 ug/1 -0.03 29) Phenanthrene-dlO 25.73 188 692355 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 470299 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 321577 20.00 ug/1 -0.04
System Monitoring Compounds 37) 2,4-DDD 30.81 235 35786 5.15 ug/mL 0.31 Spiked Amount 5.000 Recovery = 103.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.03 128 782 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.76 149 329 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0208.M Thu Feb 21 12:37:20 2002 Page 1
NYC-WTC_000052861
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