NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS analysis results for sample AE02601, Mar 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AE02601 conducted on March 7, 2002, including surrogate recovery data.
NYC-WTC_000005344–000005353Folder label: “GCMS X 2/5/02 A 3/1/02”
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NYC 9/11 Public Portal Document QUdIlL LdLLOI KepOL L (91 KeviEwed)
Data File C:\HPCHEM\l\DATA\MAR0102\2601.D Vial: 11 Acq On 1 Mar 2002 6:12 pm Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 4 11:27 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via DataAcq Meth : : Initial Calibration GCMS0208 ] 6C Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.32 152 305428 20.00 ug/1 -0.04 10) Naphthalene-d8 15.95 136 1187428 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 630595 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.71 188 911963 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 639353 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 435328 20.00 ug/1 -0.07
System Monitoring Compounds 37) 2,4-DDD 30.79 235 59772 6.28 ug/mL 0.29 Spiked Amount 5.000 Recovery = 125.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.75 149 979 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 2601.D GCMS0208.M Mon Mar 04 11:29:06 2002 Page 1
NYC-WTC_000005346
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