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GCMS analysis results for sample AE01330, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01330 conducted on February 27, 2002.

NYC-WTC_000052868–000052874

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB1902\1330.D Vial: 15 Acq On : 19 Feb 2002 11:59 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\l\METHQDS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Carbon dioxide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

45.52 0.52 ug/1 22594 Perylene-dl2 38.07

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbon dioxide 44 CO2 000124-38-9 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Ethyne, fluoro- 44 C2HF 002713-09-9 3 4 Nitrous Oxide 44 N20 010024-97-2 2 Abundance ' Scan 4409 (45.519 min): 1330.D (-) m/z 39.95 100.00% 43

5000 ! T 45.20 45.40 45.60 45.80 ................................. 208...... 233 . 31 ■ ' ■ ' i ' ' m/z 43.95 54.69% m-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62263: Carbon dioxide 44

5000 45.20 45.40 45.60 45.80

16 m/z 35.90 1.19%

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 29 44 .

45.20 45.40 45.60 45.80 5000 m/z 44.95 0.93%

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #35: Ethyne, fluoro- 44 45.20 45.40 45.60 45.80 m/z 253.05 0.65% 5000- 31

m/z-> 44 20 40 60 80 100 120 140 160 180 200 220 240 260 280 • • i ■ TII 45.20 45.40 45.60 45.80

1330.D GCMS0208.M Thu Feb 21 15:25:24 2002 Page 1

NYC-WTC_000052873

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NYC-WTC_000052873Source: NYC Law Department, mirrored locally

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