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GCMS analysis results for sample AE01043, Feb 2002

Machine-extracted title · confidence 50%

GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.

NYC-WTC_000052832–000052847

Folder label: “GCMS X 1/17/02 A 2/16/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB1502\1043.D Vial: 29 Acq On : 16 Feb 2002 8:32 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Carbon dioxide Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

43.54 0.47 ug/1 24828 Perylene-dl2 38.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbon dioxide 44 CO2 000124-38-9 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Ethylene oxide 44 C2H40 000075-21-8 3 4 Ethyne, fluoro- 44 C2HF 002713-09-9 3 Abundance ( Scan 4194 (43.543 min): 1043.D ( ) m/ z 39.95100.00% 40

5000

43.20 43.40 43.60 43.80 • ■ i • > ... 78 209 253281 m/ z 43.95 50.33% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #34: Carbon dioxide 44

5000 43.20 43.40 43.60 43.80 m/z 44.95 1.14% 16 - miz-20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 29 44 . T 43.20 43.40 43.60 43.80 5000 m/z 35.90 0.91%

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62266: Ethylene oxide 29 43.20 43.40 43.60 43.80 15 44 m/z 252.85 0.72% 5000

m/z-> mip 20 40 60 80 i ■'1 ■ i ■ 1 1 ' 111 1 ‘I"CIB"F 100 120 140 160 180 200 220 240 260 280 J will m 1 ' ' ' ■ ' ' • I ' ' 1 ■ I ' ' ' ’ 43.20 43.40 43.60 43.80

1043.D GCMS0208.M Wed Feb 20 14:29:37 2002 Page 8

NYC-WTC_000052846

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NYC-WTC_000052846Source: NYC Law Department, mirrored locally

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