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GCMS analysis results for sample AE00844, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052291–000052310

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052295
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP020702.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.499 9 11 15 rBV 39222 50567 0.40% 0.074% 2 3.613 19 21 25 rBV 38178 55699 0.44% 0.082% 3 3.922 43 48 51 rVB 19013 30095 0.24% 0.044% 4 5.920 221 223 227 rBV 79155 152908 1.20% 0.224% 5 6.011 227 231 235 rW 56888 113007 0.88% 0.166%

6 6.091 235 238 249 rVB 9397 27178 0.21% 0.040% 7 9.562 539 542 547 rBV2 9866 26690 0.21% 0.039% 8 9.710 551 555 561 rW 4137250 7933893 62.05% 11.636% 9 9.859 565 568 581 rW 17821 68721 0.54% 0.101% 10 13.192 855 860 865 rBV 5809778 11051978 86.44% 16.210%

11 13.375 873 876 891 rVB2 10545 32083 0.25% 0.047% 12 18.341 1305 1311 1315 rBV 5754906 11801624 92.30% 17.309% 13 22.280 1653 1656 1661 rW 39694 83612 0.65% 0.123% 14 22.634 1681 1687 1693 rBV2 5625543 12785490 100.00% 18.752% 15 22.771 1697 1699 1721 rVB 97387 387375 3.03% 0.568%

16 27.726 2127 2133 2139 rW 1131151 2077589 16.25% 3.047% 17 30.489 2369 2375 2409 rBV2 5021090 12138430 94.94% 17.803% 18 31.105 2419 2429 2433 rBV4 11187 36595 0.29% 0.054% 19 34.416 2713 2719 2747 rBV 3261949 9299688 72.74% 13.640% 20 34.941 2761 2765 2769 rVB2 11263 28367 0.22% 0.042%

Sum of corrected areas: 68181589

00844.D HP020702.M Thu Feb 21 09:58:15 2002 Page 1

NYC-WTC_000052295

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NYC-WTC_000052295Source: NYC Law Department, mirrored locally

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