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GCMS analysis results for sample AE00842, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.

NYC-WTC_000052251–000052270

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052255
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00842.D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: ■ Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP020702.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 5 10 15 rBV 45072 79931 0.60% 0.111% 2 3.613 19 21 25 rBV 40695 58894 0.44% 0.082% 3 3.773 31 35 45 rW3 9795 39480 0.30% 0.055% 4 3.922 45 48 53 rVB2 17409 32960 0.25% 0.046% 5 5.920 219 223 227 rBV 92010 172569 1.30% 0.240%

6 6.011 227 231 235 rVB 75111 147393 1.11% 0.205% 7 9.562 537 542 547 rBV 17727 44022 0.33% 0.061% 8 9.710 551 555 561 rW 4155906 8159577 61.26% 11.327% 9 9.847 565 567 575 rBV 20182 52151 0.39% 0.072% 10 13.192 855 860 865 rBV 6001052 11412355 85.68% 15.843%

11 14.334 957 960 969 rVB4 8915 31120 0.23% 0.043% 12 18.341 1305 1311 1315 rBV 6147701 12308829 92.41% 17.088% 13 22.280 1653 1656 1661 rW 44707 89734 0.67% 0.125% 14 22.634 1681 1687 1693 rBV2 5715375 13319274 100.00% 18.490% 15 22.771 1697 1699 1729 rVB 100945 451044 3.39% 0.626% 16 27.543 2111 2117 2127 rBV 28590 67550 0.51% 0.094% 17 27.726 2127 2133 2139 rBV 1288903 2311270 17.35% 3.209% 18 30.489 2369 2375 2381 rBV2 5278449 12646256 94.95% 17.556% 19 31.105 2419 2429 2447 rVB5 26173 118534 0.89% 0.165% 20 34.416 2713 2719 2753 rBV 3821865 10490437 78.76% 14.563%

Sum of corrected areas: 72033380

00842.D HP020702.M Thu Feb 21 09:58:08 2002 Page 1

NYC-WTC_000052255

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NYC-WTC_000052255Source: NYC Law Department, mirrored locally

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