GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\01138.D Vial: 4 Acq' On : 25 Feb 2002 1:43 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.498 9 11 15 rVB 25641 36120 0.29% 0.056% 2 3.622 17 22 33 rBV 35556 60162 0.49% 0.093% 3 3.927 45 49 57 rVB 17255 33088 0.27% 0.051% 4 4.378 85 89 97 rVB 25313 38277 0.31% 0.059% 5 5.948 225 228 231 rBV 46958 97841 0.80% 0.152%

6 6.004 231 233 239 rVB 46770 91872 0.75% 0.142% 7 6.580 277 284 295 rVB3 9472 35555 0.29% 0.055% 8 7.122 325 332 337 rBV 8207 22648 0.18% 0.035% 9 9.718 557 562 567 rBV 3806908 7693935 62.69% 11.924% 10 9.887 573 577 591 rVB2 8233 42544 0.35% 0.066%

11 12.540 809 812 815 rVB 30244 47747 0.39% 0.074% 12 13.195 865 870 875 rBV 5711688 11191672 91.19% 17.344% 13 13.376 883 886 897 rVB2 10977 32184 0.26% 0.050% 14 18.331 1319 1325 1331 rBV 5837304 11773199 95.93% 18.245% 15 22.283 1669 1675 1681 rVB2 34639 71459 0.58% 0.111%

16 22.633 1701 1706 1711 rBV2 5611290 12272741 100.00% 19.020% 17 24.845 1897 1902 1913 rVB 15814 41793 0.34% 0.065% 18 27.724 2151 2157 2163 rW 826066 1429377 11.65% 2.215% 19 30.490 2397 2402 2441 rBV 4477497 10908214 88.88% 16.905% 20 34.407 2743 2749 2787 rBV 3181976 8606691 70.13% 13.338%

Sum of corrected areas: 64527119

01138.D HP022102.M Tue Feb 26 08:30:02 2002 Page 1

NYC-WTC_000003467