GCMS analysis results for sample AE00472, Feb 26 2002

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Data File : C:\MSDCHEM\l\5973N\02FEB07\00472A.D Vial: 3 Acq On : 7 Feb 2002 12:42 pm Operator: Sample : 508 scan re-ext. Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1,1'-oxybis- (C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

9.55 0.13 ug/L 55439 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 -Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 40 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 9 3 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 4 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 9 Abundance Scan 541 (9.550 min): 00472A.D (-) m/z 59.10 100.00% 59

5000

O' i ■ 1 1 1 r ----- 45 73 103

i-i ‘mn 9.20 m/z 9.40 45.10 M_ 9.60 9.80 40.79% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29204:2-Propanol, 1.1'-oxybis- (CAS) $$ Dipropylene glyc... 50

5000: 31 45 9.20 9.40 9.60 19.80 T8 103 m/z 103.10 38.15%

n/z-> 0 ■ i ■ 1 ■ 1I■ • ■ ■i 20 30 40 ...... l pi 70 80 90 100 110 120 130 140 50 60 Abundance #61826: 2-Butanol, 3,3‘-oxybis- 50 —

9.20 9.40 9.60 9.80 5000: 31 m/2 73.10 28.24% 45 103

.................................................... 134 0 11 " 4, r - 7 4 1 r 1— /z-> Abundance 20 30

31 40 50 (60 70 80 90 100 110 120 130 140 #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 50 9.20 9.40 ANA 9.60 9.80 V

m/z 41.10 26.31%

m/z—> 5000

39 . 99

40 45

0 > । । । 1 । 1 —4l-l- r All. 20 30 50 60 70 75 80 90 103

100 110 120 130 140 9.20 9.40 y 9.60 9.80 "IT

00472A.D HP020702.M Thu Feb 21 09:57:54 2002 Page 9

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