GCMS analysis results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00842.D Vial: 6 Acq On : 7 Feb 2002 6:34 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Butanoic acid, 3-oxo-, 1,1-.. Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

14.33 0.05 ug/L 31120 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, 3-oxo-, 1,1-dimet... 158 C8H14O3 001694-31-1 9 2 Hexylene Glycol 118 C6H14O2 000107-41-5 9 3 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4 4 1-Hexanamine 101 C6H15N 000111-26-2 4 Abundance Scan 960 (14.334 min): 00842.D (-) m/z 59.10 100.00% 59

5000 41 103 85 14.00 14.20 14.40 14.60 Of ■ ।' ■ ■ ■ । ■11 rb ‘1 ■ । ' ’ I ।।।, TT m/z 41.10 33.08% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 A Abundance #57471: Butanoic acid, 3-oxo-, 1.1-dimethylethyl ester (CA... L 59

43 5000 84 14.00 14.20 14.40 14.60 69 m/z 103.10 29.83% 103 29 01 ......... I 11 ■'' ■ i ■ I T —l I ■ i • • ■ • i ■ TBT I ' ■ ■ 158 i ■' ■ ■ i ■' ■' i'' '' i ■''11 ■ m/z-> 20 30 40 5060 70 80 90 100 110 120 130 140 150 160 Abundance #17793: Hexylene Glycol 43 59 ■ • i ■ 14.00 14.20 14.40 14.60 5000 m/z 45.10 29.14% 31 85 103

■n/z--> 0 ■ ।■■■■।■■■■। 20 30 40 ‘ I’’ 50 60 ■ । • i ■ ■ ■ ■ i ■ 70 80 90 100 110 120 + i' ■ ■ ■ i ■ ■ ■11 ■ ■ ■ ■ i' ■ ■ ■ I 130 140 150 160 Abundance #500: 2-METHYL-3.3-D2-AZIRIDINE T’I 29 58 14.00 14.20 14.40 14.60 m/z 57.00 26.58%

5000 U 42

m/z-> o ■ i ■' 20 30 Mu 40 50 60 70 80 90 < i. ■ ■ • । ■ •. ■ ।. ■ ■ ■ । • ■. ■ । • ■ ■ ■ । 100 110 120 130 140 150 160 IT 4 14.00 14.20 14.40 14.60 ‘I

00842.D HP020702.M Thu Feb 21 09:58:09 2002 Page 11

NYC-WTC_000052265