GCMS analysis results for sample AE03247, March 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 • Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

3.62 0.09 ug/L 38566 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 4 Abundance

n/z-> Butanoic

5000

10 ,w *

0- ■ ' i ■ 1 ■ ■ i 1 ■ ■ ■ । 1 ■ 1 ' i 20 acid,

30 40 methyl lean 22 (3.622 min): 03247. D (-) 43

50 ester (CAS... 102 C5H10O2

59

।..... I,,...... ! 60 70 74

87

■ 1 i ■ PP—1 i ■ ■ ■ ■ i 80 90 100 110 m/ z

MAAMAAA 000623-42-7 83 43.10 100.00%

3.50 3.60 3.70 3.80 3.90 4.00 m/ z 74.00 94.90% Abundance #9218: Butanoic acid, methyl ester 43 74

5000 27 3.50 3.60 3.70 3.80 3.90 4.00 15 59 m/z 71.10 68.45% 87 33 102 0- 1 ' i ■ ■ ■ ■ i 1 ■ ■ ' i ■ i 11/020/, — ———————————— /z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 i1 " ' i . A r,i11 3.50 3.60 3.70 3.80 3.90 4.00 5000 m/ Z 41.10 39.94% 59 87 69 102 0- 1 ' i ' ' ' ' i ‘ ' i ■ ' ' ' i + 1 ’1 ■ ■ । • • • • । ■ ■ • ■ । ■ 1 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9217: Butanoic acid, methyl ester 43 74 3.50 3.60 3.70 3.80 3.90 4.00 m/z 59.00 29.77%

5000 27 59 87 33 | 102 0 IIIInIIIIIIIII‘un‘/n“* ——— TTT III III I I I I’II I I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90 4.00

03247.D HP022102.M Mon Mar 04 12:33:20 2002 Page 3

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