GCMS analysis results for sample AE03245, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

NYC-WTC_000006085–000006104

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03245.D Vial: 6 • Acq On : 1 Mar 2002 2:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.62 0.13 ug/L 57614 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid,. methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid. methyl ester 102 C5H10O2 000623-42-7 83 Abundance Scan 22 (3.622 min): 03245.D (-) m/ z 43.10 100.00% 74

5000

N 59 87 i ‘ ‘ 1111111 mA/W./) 3.50 3.60 3.70 3.80 3.90 4.00 O— । i 51 J |............| —————————————— m/ z 74.00 83.35% ■ i ' 1 ■ 1 i 1 ■ 1 ' r 1 1 1 1 1 1 1 1 1 1 1 1 ‘ 1 1 lz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9220: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43

15 74 5000 27 i''1' i' ■ ■ ■ i'1'' i'1'11 3.50 3.60 3.70 3.80 3.90 4.00 59 m/ Z 71.00 59.94% 87 o1 1 1 i 1 ' 1 ■ i ' 1 1 ' i 33 P 00000—01—— | 102 1 1 i 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 T-q-TT 3.50 3.60 3.70 3.80 3.90 4.00 5000 m/z 41.10 30.86% 59 87

m/z-> Abundance 33 0- 1 ' i ■ ' 1 ' i ' 1 ■ ' i ''■ ■ ■ i 10 20 30 40

43 50 60 70 #9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 74 80 90 102 100 110 AAA. ■ ■ ■ । 3.50 3.60 3.70 3.80 3.90 4.00 m/ z .

59.00 M 27.10%

5000 59 87 69 102 0-PP I'l ' I ' 1 1 ' 1 1 ' TTT 11 I 1 1 11 I ' 1 1 1 I'1 1 1 1 I ■ ■ i ■' m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90 4.00

)3245.D HP022102.M Mon Mar 04 12:33:05 2002 Page 3

NYC-WTC_000006091

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