GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 . Acq On : 16 Jan 2002 2:11 pm perator : Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 17 08:12:17 2002 Quant Results File: SCAN508.RES

Quant Method Title : : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) 508 scan method Wo J y Last Update Response via DataAcq Meth : : :

Internal Standards Fri Jan 11 13:20:07 2002 Initial Calibration SCAN508

R.T. Qlon Response VW N Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1290915 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 5524078 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2951497. 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 4919254 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4262076 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3074544 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 435285 5.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 112.00%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 10474 0.19 ug/L # 9 20) Dimethylphthalate 18.34 163 472767 2.43 ug/L + 56 21) 2,6-Dinitrotoluene 18.34 165 375396 9.87 ug/L # 17 35) Di-n-butylphthalate 24.85 149 28686 0.09 ug/L 98 41) Benzo(a)anthracene 30.50 228 10408 0.04 ug/L # 58 42) Bis(2-ethylhexyl)phthalate 31.11 149 187171 1.43 ug/L 98 43) Chrysene 30.50 228 10408 0.04 ug/L # 56 45) Di-n-octylphthalate 32.84 149 6960 0.02 ug/L # 74 48) Benzo(a)pyrene 34.42 252 10415 0.05 ug/L # 1

(#) = qualifier out of range (m) = manual integration 00700.D SCAN508.M Thu Jan 17 08:12:17 2002 Page 1

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