GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
NYC-WTC_000051794–000051805Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LALLCLY bedrcr compound Keporc
Data File : C:\MSDCHEM\1\5973N\02JAN16\0110B.D Vial: 1 . Acq On : 16 Jan 2002 10:50 am Operator: Sample : lab blank 1/10 Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 4 Morpholine $$ p-Isoxazine, . Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 8.24 0.15 ug/L 43058 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Morpholine $$ p-Isoxazine, tetra... 87 C4H9NO 000110-91-8 38 2 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 25 3 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 9 4 Morpholine (CAS) $$ BASF 238 $$ ... 87 C4H9NO 000110-91-8 9 Abundance Scan 426 (8.237 min): 0110B.D (-) m/z 57.10 100.00% 45 57
5000 87 41
7.80 8.00 8.20 8.40 8.60 m/z—> 0b ' 171 I I | I V | | | v —l 49 Hm If 1" 1 * " 11" '' p 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 84 H J7™ I ■' m/ z 45.10 96.69% Abundance #4374: Morpholine $$ p-Isoxazine, tetrahydro- $$ BASF 238 ... 23 57
5000 87 .................... .......... 7.80 8.00 8.20 8.40 8.60 42 m/z 87.10 48.43% 54 n/z-> — 0b '' I " ’' I'1'' I " "I' 5 —H —mmmmmmmmm HTTTTTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4372: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide ... 29 57 7.80 8.00 8.20 8.40 8.60 5000 m/z 56.10 37.29% 87 15 26 42 Oh ■ u ” " i' ‘111117 «r "1 ■ i" " i''" ।।" I HTTTTTTTTTT n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4376: Morpholine (CAS) $$ BASF 238 $$ Diethylene oximide ... ITt ‘EId'I'I'." 57 7.80 8.00 8.20 8.40 8.60 87 m/ Z 41.10 34.25%
5000
m/z-> Of 5 -------+45,54 +Tpr +1TTTTTTTTUTTTTWTTTTTTTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60
110B.D SCAN508.M Thu Jan 17 09:46:05 2002 Page 6
NYC-WTC_000051802
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000051674
Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050627
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052233
Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051531
Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051624
Laboratory report showing GCMS analysis results for sample AE00615 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003425
Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.
2 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051806
GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.
Filed in the same folder