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GCMS analysis results for sample AE00559, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.

NYC-WTC_000051727–000051739

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN15\00559.D Vial: 3 Acq On : 15 Jan 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:54 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1086407 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4633011 20.00 ug/L -0.02 17) Acenaphthene-dlO 18.34 164 2379772 20.00 ug/L -0.01 29) Phenanthrene-dlO 22.63 188 3995310 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3551639 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2531129 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 314277 4.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.60%

Target Compounds 95100/0.21 ug/L Qvalue 2) n-Nitrosodimethylamine 3.60 74 12 20) Dimethylphthalate 18.34 163 381806 ' 2.43 ug/L 56 21) 2,6-Dinitrotoluene 18.34 165 299891 ,9.78 ug/L 17 25) Diethylphthalate 20.00 149 19563 0.13 ug/L 98 33) Phenanthrene 22.69 178 10495 / 0.05 ug/L 97 34) Anthracene 22.69 178 10495 /■ 0.05 ug/L 97 35) Di-n-butylphthalate 36) Fluoranthene 24.85 26.22 149 202 93209 21050 1 0.36 ug/L 0.10 ug/L 95 91 3 9) Pyrene 26.85 202 22490 . 3 0.08 ug/L 94 40) Butylbenzylphthalate 29.24 149 7958. 1 0.06 ug/L 97 41) Benzo(a)anthracene 30.47 228 33533 AR 0.16 ug/L 97 42) Bis(2-ethylhexyl)phthalate 31.11 149 42323 V 0.79 ug/L 94 43) Chrysene 30.56 228 38785 \ 0.19 ug/L 94 45) Di-n-octylphthalate 32.82 149 5494 \ 0.02 ug/L # 74 46) Benzo(b)fluoranthene 33.50 252 9127 0.05 ug/L 93 47) Benzo(k)fluoranthene 33.50 252 9127 0.05 ug/L 92 48) Benzo(a)pyrene 34.42 252 18019 011 ug/L # 1 51) Benzo(g,h,i)perylene 37.70 276 5194 0.04 ug/L 4 49

(#) = qualifier out of range (m) = manual integration 00559.D SCAN508.M Tue Jan 15 15:51:55 2002 Page 1

NYC-WTC_000051729

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NYC-WTC_000051729Source: NYC Law Department, mirrored locally

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