GCMS blank analysis for sample AE00365, Jan-Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\0109B.D Vial: 1 Acq On : 15 Jan 2002 10:12 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rVB 20983 33390 0.33% 0.063% 2 3.990 49 54 59 rW 6726 16384 0.16% 0.031% 3 4.630 107 110 117 rVB4 10301 19789 0.20% 0.038% 4 4.846 123 129 141 rBV3 11101 45344 0.45% 0.086% 5 5.006 141 143 149 rVB3 15503 24226 0.24% 0.046%

6 5.509 183 187 203 rBV3 5012 29357 0.29% 0.056% 7 5.885 217 220 247 rBV 607326 1293735 12.93% 2.456% 8 9.721 551 556 563 rBV 2764506 5631050 56.28% 10.692% 9 13.192 855 860 865 rBV 4161139 8016142 80.12% 15.221% 10 18.341 1305 1311 1315 rBV 4670952 9036412 90.32% 17.158%

11 22.280 1651 1656 1659 rW2 31855 60651 0.61% 0.115% 12 22.634 1681 1687 1693 rW2 4510280 10005198 100.00% 18.997% 13 22.771 1695 1699 1717 rW 54030 180697 1.81% 0.343% 14 23.045 1719 1723 1731 rW 3561 15273 0.15% 0.029% 15 24.849 1877 1881 1887 rW 48100 93479 0.93% 0.177%

16 27.726 2129 2133 2139 rW 772538 1365151 13.64% 2.592% 17 29.667 2299 2303 2313 rVB3 5574 15041 0.15% 0.029% 18 30.489 2369 2375 2381 rBV2 4021217 9295016 92.90% 17.649% 19 34.416 2713 2719 2745 rBV 2847417 7468978 74.65% 14.182% 20 37.168 2957 2960 2969 rBV5 4090 21112 0.21% 0.040%

Sum of corrected areas: 52666425

0109B.D SCAN508.M Wed Jan 16 08:14:16 2002 Page 1

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