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GCMS blank results for sample AE00703, Jan 16 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.

NYC-WTC_000051794–000051805

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051797
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\0110B.D Vial: 1 Acq On : 16 Jan 2002 10:50 am Operator: Sample : lab blank 1/10 Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.602 15 20 25 rBV 19899 38796 0.39% 0.074% 2 4.618 107 109 121 rVB3 7068 26329 0.27% 0.050% 3 4.858 125 130 137 rBV4 10887 41640 0.42% 0.079% 4 5.006 137 143 151 rVB 13310 27725 0.28% 0.053% 5 5.885 215 220 249 rVB 534728 1285509 13.03% 2.441%

6 7.450 353 357 373 rBV 34300 121050 1.23% 0.230% 7 8.237 423 426 435 rBV2 17605 43058 0.44% 0.082% 8 9.653 541 550 551 rBV3 5560 17561 0.18% 0.033% 9 9.710 551 555 563 rW 2976912 5929484 60.09% 11.259% 10 9.859 563 568 577 rW2 7168 24027 0.24% 0.046%

11 10.098 587 589 597 rVB3 12216 26637 0.27% 0.051% 12 13.192 855 860 865 rBV 4562505 8485090 85.98% 16.111% 13 18.341 1305 1311 1315 rBV 4770673 9311168 94.36% 17.680% 14 22.280 1653 1656 1661 rVB2 31520 54942 0.56% 0.104% 15 22.634 1681 1687 1693 rBV2 4549121 9868198 100.00% 18.737%

16 22.771 1695 1699 1707 rVB 47031 122570 1.24% 0.233% 17 27.726 2129 2133 2139 rBV 764088 1329837 13.48% 2.525% 18 30.489 2369 2375 2381 rBV2 3905314 8753376 88.70% 16.621% 19 34.416 2713 2719 2757 rBV 2621776 7141052 72.36% 13.559% 20 37.522 2985 2991 2995 rBV6 4343 18087 0.18% 0.034%

Sum of corrected areas: 52666136

110B.D SCAN508.M Thu Jan 17 09:46:04 2002 Page 1

NYC-WTC_000051797

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NYC-WTC_000051797Source: NYC Law Department, mirrored locally

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