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GCMS blank results for sample AE00277, Jan 2002

Machine-extracted title · confidence 90%

Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.

NYC-WTC_000050825–000050837

Folder label: “GCMS X 1/7/02 A 1/9/02

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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN09\0107BLA.D Vial: 1 Acq On 9 Jan 2002 5:19 pm Operator: Sample : lab blank 1/7 a Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.591 15 19 25 rBV 27218 54247 0.40% 0.072% 2 4.618 107 109 123 rVB6 13599 55659 0.41% 0.074% 3 4.847 123 129 139 rBV2 23828 93667 0.69% 0.124% 4 5.886 217 220 243 rBV 833476 2006837 14.86% 2.651% 5 9.082 493 500 507 rW3 15328 57356 0.42% 0.076%

6 9.254 511 515 521 rBV3 22106 64981 0.48% 0.086% 7 9.710 551 555 563 rW 4019946 8120862 60.15% 10.729% 8 10.235 595 601 613 rVB4 18220 83160 0.62% 0.110% 9 13.192 855 860 865 rBV 6462046 11737479 86.93% 15.507% 10 17.885 1265 1271 1275 rVB3 18043 55106 0.41% 0.073%

11 18.341 1305 1311 1315 rW 6483992 12648757 93.68% 16.710% 12 18.421 1315 1318 1323 rW 46974 91591 0.68% 0.121% 13 19.997 1451 1456 1463 rW3 20720 73507 0.54% 0.097% 14 22.280 1651 1656 1661 rVB2 44537 86311 0.64% 0.114% 15 22.634 1681 1687 1693 rBV2 6234722 13501627 100.00% 17.837%

16 22.771 1695 1699 1715 rVB2 63410 227457 1.68% 0.300% 17 24.849 1877 1881 1887 rW 114730 222822 1.65% 0.294% 18 27.726 2129 2133 2139 rBV 1211585 2135545 15.82% 2.821% 19 30.489 2369 2375 2381 rBV2 5580976 13204290 97.80% 17.444% 20 34.416 2713 2719 2747 rBV 4562000 11172400 82.75% 14.760%

Sum of corrected areas: 75693661

107BLA.D SCAN508.M Thu Jan 10 11:51:31 2002 Page 1

NYC-WTC_000050829

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NYC-WTC_000050829Source: NYC Law Department, mirrored locally

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