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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051322
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.886 217 220 251 rBV 583036 1338078 2.89% 1.220% 2 9.539 539 540 545 rBV2 23945 59307 0.13% 0.054% 3 9.630 545 548 551 rW 26940 67114 0.14% 0.061% 4 9.710 551 555 563 rW 3207994 6665000 14.38% 6.076% 5 9.847 563 567 577 rVB2 30438 108727 0.23% 0.099%

6 13.192 855 860 865 rBV 5018847 9381773 20.24% 8.553% 7 18.341 1305 1311 1315 rBV 5271506 10247408 22.11% 9.342% 8 18.730 1339 1345 1367 rBV 100881 529744 1.14% 0.483% 9 22.280 1651 1656 1661 rBV 47409 84948 0.18% 0.077% 10 22.634 1681 1687 1693 rBV2 4758453 10917368 23.56% 9.953%

11 22.828 1693 1704 1727 rVB2 187734 1205380 2.60% 1.099% 12 23.422 1745 1756 1765 rBV3 18618 97397 0.21% 0.089% 13 23.696 1765 1780 1785 rBV6 12128 79691 0.17% 0.073% 14 24.860 1877 1882 1887 rBV2 22864 72651 0.16% 0.066% 15 26.139 1977 1994 1999 rVB 7179827 46345705 100.00% 42.250%

16 27.726 2129 2133 2139 rBV 835385 1492159 3.22% 1.360% 17 30.489 2369 2375 2381 rBV2 4624757 10936407 23.60% 9.970% 18 31.094 2425 2428 2455 rVB7 19213 141370 0.31% 0.129% 19 33.400 2625 2630 2645 rBV 138848 515064 1.11% 0.470% 20 34.416 2713 2719 2745 rBV 3607544 9408958 20.30% 8.577%

Sum of corrected areas: 109694249

00468.D SCAN508.M Fri Jan 11 10:08:42 2002 Page 1

NYC-WTC_000051322

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NYC-WTC_000051322Source: NYC Law Department, mirrored locally

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