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GCMS surrogate recovery results for sample AE00316, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.

NYC-WTC_000050963–000050976

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050968
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN10\00316.D Vial: 3 Acq On : 10 Jan 2002 10:07 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rBV 25971 42044 0.42% 0.076% 2 4.846 123 129 139 rBV3 18501 66357 0.66% 0.119% 3 5.006 139 143 149 rVB 30076 57471 0.57% 0.103% 4 5.885 217 220 227 rBV 713085 1441433 14.35% 2.594% 5 9.036 491 496 507 rBV3 33085 83812 0.83% 0.151%

6 9.562 539 542 551 rBV4 8893 43185 0.43% 0.078% 7 9.710 551 555 561 rW 3047171 6171432 61.42% 11.106% 8 13.192 855 860 865 rBV 4687941 8853174 88.11% 15.931% 9 13.580 889 894 899 rVB 20397 40123 0.40% 0.072% 10 17.885 1267 1271 1279 rVB2 27110 50763 0.51% 0.091%

11 18.341 1305 1311 1315 rW 4956539 9611641 95.66% 17.296% 12 19.997 1453 1456 1463 rVB 45843 90460 0.90% 0.163% 13 22.280 1653 1656 1661 rVB2 37394 66884 0.67% 0.120% 14 22.634 1681 1687 1693 rBV2 4484519 10047660 100.00% 18.081% 15 22.771 1695 1699 1701 rW 39138 62323 0.62% 0.112%

16 23.422 1753 1756 1761 rW 19451 38419 0.38% 0.069% 17 27.726 2127 2133 2139 rW 912912 1611707 16.04% 2.900% 18 30.489 2369 2375 2381 rBV2 4035498 9458370 94.14% 17.020% 19 31.105 2425 2429 2447 rW 54335 190227 1.89% 0.342% 20 34.416 2713 2719 2737 rBV 2910294 7543210 75.07% 13.574%

Sum of corrected areas: 55570695

30316.D SCAN508.M Thu Jan 10 11:52:11 2002 Page 1

NYC-WTC_000050968

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NYC-WTC_000050968Source: NYC Law Department, mirrored locally

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