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GCMS surrogate recovery results for sample AE00278, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.

NYC-WTC_000050856–000050874

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050861
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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\5973N\02JAN09\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: ■ Sample 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.476 7 9 17 rVB 56155 90819 0.50% 0.092% 2 4.835 125 128 135 rBV2 40221 106061 0.58% 0.108% 3 5.885 217 220 227 rW 1056539 2186351 12.00% 2.221% 4 6.000 227 230 243 rVB 105631 287362 1.58% 0.292% 5 9.722 551 556 561 rW 5011857 9836660 53.99% 9.990%

6 13.192 855 860 865 rBV 7441560 14038173 77.06% 14.258% 7 18.341 1305 1311 1315 rBV 8293449 15882590 87.18% 16.131% 8 19.997 1451 1456 1461 rVB 99726 195346 1.07% 0.198% 9 22.280 1653 1656 1661 rVB 75016 130434 0.72% 0.132% 10 22.634 1681 1687 1693 rBV2 7794735 17729480 97.32% 18.006%

11 22.771 1695 1699 1703 rVB 76411 125295 0.69% 0.127% 12 27.543 2111 2117 2121 rBV 51308 109947 0.60% 0.112% 13 27.726 2127 2133 2139 rBV 1748497 3162819 17.36% 3.212% 14 30.500 2369 2376 2381 rBV 7664266 18218068 100.00% 18.503% 15 31.105 2425 2429 2435 rW2 28493 91811 0.50% 0.093%

16 33.263 2613 2618 2627 rBV7 25608 104235 0.57% 0.106% 17 34.119 2687 2693 2709 rBV3 42992 182977 1.00% 0.186% 18 34.416 2713 2719 2745 rW2 6111383 15784485 86.64% 16.031% 19 34.941 2761 2765 2773 rBV2 33085 110239 0.61% 0.112% 20 35.741 2831 2835 2845 rBV2 29112 88498 0.49% 0.090%

Sum of corrected areas: 98461650

278.D SCAN508.M Thu Jan 10 11:51:43 2002 Page 1

NYC-WTC_000050861

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NYC-WTC_000050861Source: NYC Law Department, mirrored locally

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