GCMS surrogate recovery results for sample AE00282, Jan 2002

NYC 9/11 Public Portal Document Data File C:\MSDCHEM\l\5973N\02JAN09\282.D Vial: 7 Acq On 9 Jan 2002 11:12 pm Operator: . Sample 508 scan ext 1/7 Inst : Instrumen Mise January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 26055 53155 0.40% 0.072% 2 3.899 41 46 51 rVB2 12956 28346 0.21% 0.038% 3 4.230 71 75 83 rBV7 10101 36441 0.27% 0.049% 4 4.629 101 110 121 rBV7 13517 54547 0.41% 0.073% 5 4.858 121 130 139 rBV4 18592 70893 0.53% 0.096%

6 5.006 139 143 151 rVB3 17450 45032 0.34% 0.061% 7 5.543 181 190 193 rBV4 6118 25776 0.19% 0.035% 8 5.885 217 220 247 rVB 801323 2053820 15.34% 2.767% 9 9.573 541 543 547 rW3 11917 33094 0.25% 0.045% 10 9.710 551 555 563 rW 3545596 7864857 58.75% 10.596%

11 9.858 563 568 577 rW2 18323 65328 0.49% 0.088% 12 13.192 855 860 865 rBV 6038354 11312235 84.50% 15.240% 13 18.341 1305 1311 1315 rBV 6452404 12427646 92.83% 16.743% 14 22.280 1651 1656 1661 rW2 43645 86845 0.65% 0.117% 15 22.634 1681 1687 1693 rBV2 6259090 13239674 98.90% 17.837%

16 22.771 1695 1699 1711 rVB 64594 186038 1.39% 0.251% 17 27.726 2129 2133 2139 rBV 1088248 1940567 14.50% 2.614% 18 30.489 2369 2375 2381 rBV2 5972732 13387454 100.00% 18.036% 19 31.105 2425 2429 2437 rW2 24145 67565 0.50% 0.091% 20 34.416 2713 2719 2739 rW 4426750 11247862 84.02% 15.153%

Sum of corrected areas: 74227175

282.D SCAN508.M Thu Jan 10 11:52:04 2002 Page 1

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