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GCMS surrogate recovery results for sample AE00317, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.

NYC-WTC_000050977–000050993

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050982
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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN10\00317.D Vial: 4 Acq On : 10 Jan 2002 10:57 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.488 7 10 19 rVB 26721 51145 0.47% 0.083% 2 4.846 125 129 139 rBV3 14998 52005 0.47% 0.084% 3 5.006 139 143 149 rVB 52407 90439 0.82% 0.147% 4 5.702 201 204 209 rBV 26992 51462 0.47% 0.083% 5 5.885 217 220 227 rBV 840820 1623686 14.78% 2.631%

6 5.999 227 230 245 rVB 59169 169713 1.55% 0.275% 7 9.721 551 556 561 rW 3255955 6653906 60.58% 10.780% 8 13.192 855 860 865 rBV 4960644 9393454 85.52% 15.218% 9 18.341 1305 1311 1315 rBV 5285483 10055139 91.55% 16.291% 10 19.996 1451 1456 1467 rVB2 37274 85953 0.78% 0.139%

11 22.280 1651 1656 1661 rBV 42182 76371 0.70% 0.124% 12 22.645 1681 1688 1693 rBV2 4838350 10811766 98.44% 17.516% 13 22.771 1695 1699 1701 rVB 45396 68819 0.63% 0.111% 14 23.422 1751 1756 1761 rBV 35278 70576 0.64% 0.114% 15 26.207 1997 2000 2005 rVB 27467 54878 0.50% 0.089%

16 26.847 2051 2056 2061 rVB 26552 56029 0.51% 0.091% 17 27.726 2129 2133 2139 rVB 993434 1793118 16.33% 2.905% 18 30.489 2369 2375 2381 rBV 4460974 10983322 100.00% 17.794% 19 31.105 2425 2429 2443 rVB2 24143 82394 0.75% 0.133% 20 34.416 2713 2719 2745 rW 3754556 9499755 86.49% 15.391%

Sum of corrected areas: 61723930

30317.D SCAN508.M Thu Jan 10 11:52:16 2002 Page 1

NYC-WTC_000050982

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NYC-WTC_000050982Source: NYC Law Department, mirrored locally

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